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Spectrometer
LIST

FTIR Spectrometer

FTIR-761S

Product Category: FTIR

FTIR-761S is a single beam FTIR spectrometer. This instrument is operated by a PC. It is a powerful tool to analyze the sample structure in many fields such as petroleum, chemical engineering and pharmaceutical.


Products Detail Technical Parameter Feature And Application Fields Of Use Details Download

High stable optical system

The design integrates main components to an optical bench machined from a cast aluminum. Highly stable and no need for adjustment, re-moving troubles of maintenance of optical path.

Precision machinery ensures high repeatability of every scanning. Advanced design concept is adopted in both optical path and every part

●   The system’s corner cube optics provides easy operation without requiring complicated electronics and additional moving parts. In addition, many components of the spectrometer are user replaceable which saves time over the lifetime of the instrument.

Internal dynamic collimation system and movable mirror driving system keep interferometer at optimum situation. Voice-coil driver and precision slide improves the ability of working in severe conditions.

The spectrometer includes a container of desiccant that protects the beam splitter and other optical components from moisture damage.


Specifications

Wavenumber Range

7800 ~ 350 cm-1

Resolution

Superior to 0.9cm-1

Signal Noise Ratio

Superior to 50000:1 ( resolution 4cm-1; sample and background scan for 1 min 2100cm-1) RMS:250000:1

Detector

High resolution detector

Beamsplitter

Coated KBr

Light Source

Long life, air cooled IR light source

Electronic System

A/D converter of 24 bits at 500MHz, USB 2.0

Power

110-220V AC, 50-60Hz

wejght

15kg


Parts included

No.

Description

Qty

1

Spectrometer

1

2

Power Supply

1

3

Dust Cover

1

4

USB Cable

1

5

Power Cord

1

6

Screw Driver, 150x6mm

1

7

Allen Wrench, 2.5mm

1

8

Replacement Desiccant

1

9

Polystyrene Film

1

10

Software CD

1

11

User Manual

1 copy


Optional accessories

Above are some of the usual accessories, there are more things to meet the further use.

Item

Accessories

Description

Mode

1

Attenuated total reflection accessory

ATR

Pure diamond crystals are suitable for qualitative analysis of elastic polymers such as plastics and rubbers. The single ATR reflection accessory is suitable for testing samples such as solids, fibers, hard polymers, paint chips, films on glass or metal surfaces, and trace amounts of liquids, with a maximum wavelength range of 4000 to 30 waves

LA-106


For the pharmaceutical industry solutions

Compression method is a traditional method of infrared spectroscopy, only thinner, agate mortar, tablet press and tablet press can be sample preparation, is a simple and easy way.

A blank sheet made of potassium bromide or potassium chloride was used to record the spectra. The baseline should be about 75% transmittance. Except for 3440cm-1 and 1630cm-1, there was a certain absorption peak due to residual or attached water. The area should not exhibit an absorption band greater than 3% transmittance.

(1) solid powder compression method - operating procedures

① the amount of test products: about 1.0 ~ 1.5mg (drying)

② the amount of thinner: about 200 ~ 300mg (drying)

③ grinding process: full grinding (no obvious particles is appropriate)

④ Preparation of the sample: into the tablet mold, even paved, under normal pressure or vacuum production (excluding air and moisture), close the hydraulic valve, pressurized to 8 ~ 10MPa, standing 10-15s, pressed into pieces

⑤ for the test piece requirements: visual inspection should be uniform and transparent, no obvious particles.

 

(2) Note on the tablet method

① samples and diluent preparation before the need for drying (to prevent the impact of water)

② samples and potassium bromide to be grinding evenly (to prevent the scattering phenomenon)

③ compression molding after the need to slow decompression (to prevent the film cracks)

④ mold used after the first use of alcohol cotton wipe clean, and then clean, dry soft paper or soft cloth wipe clean (to prevent the mold rust)

⑤ For chlorine-containing samples, the use of potassium chloride tablet for comparison test; if the spectrum is completely consistent with the use of potassium bromide tablet, such as the spectrum is inconsistent, you must use potassium chloride tablet (to prevent ion exchange).

 

(3) Membrane method - liquid sample

Liquid samples such as various types of oil or ethanol qualitative analysis, just a small amount of stainless steel shovel to take a small amount of sample coated with potassium bromide window can be measured.


Conditions of Use

Ambient temperature: 16 ℃ ~ 25 ℃

Humidity range: 20% to 50%

Power supply: AC100V ~ 240V, 47Hz ~ 63Hz 1.2A, good grounding


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